Ni Dmg 2 2+ 3d Structure

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. In Ni(CN) 4 2-, there is Ni 2+ ion for which the electronic configuration in the valence shell is 3d 8 4s 0. In presence of strong field CN - ions, all the electrons are paired up. The empty 4d, 3s and two 4p orbitals undergo dsp 2 hybridization to make bonds with CN - ligands in square planar geometry. Mar 30, 2009  2.2. Growth of carbon nanotubes. Carbon nanotubes were produced by pyrolyzing Ni(dmg) 2 at temperatures: 750, 800, 850, 900, 950 and 1000 °C, respectively, under Ar atmosphere. In a typical experiment, a sample of Ni(dmg) 2 (0.2 g) was placed into a crucible and introduced into one end of a silica tube (ID: 20 mm, length 112 cm). The tube was.

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Nickel bis(dimethylglyoximate) is the coordination complex with the formula Ni[ONC(CH₃)C(CH₃)NOH]₂. The compound is a bright red solid. It achieved prominence for its use in the qualitative analysis of nickel.^[1]

Structure[edit]

Nickel(II) is square planar.^[2] It is surrounded by two equivalents of the conjugate base (dmgH⁻) of dimethylglyoxime (dmgH₂). The pair of organic ligands are joined through hydrogen bonds to give a macrocyclic ligand. The complex is distinctively colored and insoluble leading to its use as a chelating agent in the gravimetric analysis of nickel.

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Aprire file dmg windows 10. How to open dmg files windows 10. The use of dimethylglyoxime as a reagent to detect nickel was reported by L. A. Chugaev in 1905.^[3]

References[edit]

1. ^Greenwood, Norman N.; Earnshaw, Alan (1997). Chemistry of the Elements (2nd ed.). Butterworth-Heinemann. ISBN978-0-08-037941-8.
2. ^Donald E. Williams, Gabriele Wohlauer, R. E. Rundle (1959). 'Crystal Structures of Nickel and Palladium Dimethylglyoximes'. J. Am. Chem. Soc. 81: 755–756. doi:10.1021/ja01512a066.CS1 maint: uses authors parameter (link)
3. ^Tschugaeff, Lev (1905). 'Über ein neues, empfindliches Reagens auf Nickel' [About a new, sensitive reagent on nickel] (PDF). Berichte der deutschen chemischen Gesellschaft (in German). 38 (3): 2520–2522. doi:10.1002/cber.19050380317.

2.2 Gd

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Ni Dmg 2 2+ 3d Structure Free